Publications

Journal Articles

Enzyme-delivery Metal-organic Framework Composite Coatings for Restoration of Hyperglycemia-damaged Osteoblast Differentiation

Mitra, I., Potes, M. A., Shafi, M., Tilton, M., Elder, B. D., & Lu, L. · Biomaterials Advances · 2025

There is a significant clinical need to develop effective treatments for bone defects in patients with diabetes mellitus (DM), as they are at higher risk of fractures and impaired healing. Guided bone tissue engineering using biocompatible and biodegradable polymers is a promising approach. However, current diabetic bone regenerative therapies often fail due to the accumulation of advanced glycation products..

3D bioprinted chondrogenic gelatin methacrylate-poly(ethylene glycol) diacrylate composite scaffolds for intervertebral disc restoration

Potes, M.A., Tilton, M., Mitra, I., Liu, X., Dashtdar, B., Camilleri, E.T., Elder, B.D. and Lu, L. · International Journal of Extreme Manufacturing · 2024

Degenerative spine pathologies, including intervertebral disc (IVD) degeneration, present a significant healthcare challenge due to their association with chronic pain and disability. This study explores an innovative approach to IVD regeneration utilizing 3D bioprinting technology, specifically visible light-based digital light processing, to fabricate tissue scaffolds that closely mimic the native architecture of the IVD.

Biodegradable poly(caprolactone fumarate) 3D printed scaffolds for segmental bone defects within the Masquelet technique

Potes, M.A., Mitra, I., Hanson, K., Camilleri, E.T., Gaihre, B., Shafi, M., Hamouda, A., Lu, L. and Elder, B.D. · Journal of Orthopedic Research · 2024

Segmental bone defects, often clinically treated with nondegradable poly(methylmethacrylate) (PMMA) in multistage surgeries, present a significant clinical challenge. Our study investigated the efficacy of 3D printed biodegradable polycaprolactone fumarate (PCLF)/PCL spacers in a one‐stage surgical intervention for these defects, focusing on early bone regeneration influenced by spacer porosities.

Additively manufactured Ti–Ta–Cu alloys for the next-generation load-bearing implants

Bandyopadhyay, A., Mitra, I., Ciliveri, S., Avila, J. D., Dernell, W., Goodman, S. B., & Bose, S. · International Journal of Extreme Manufacturing · 2023

Bacterial colonization of orthopedic implants is one of the leading causes of failure and clinical complexities for load-bearing metallic implants. Topical or systemic administration of antibiotics may not offer the most efficient defense against colonization, especially in the case of secondary infection, leading to surgical removal of implants and in some cases even limbs.

Porous metal implants: processing, properties, and challenges

Bandyopadhyay, A., Mitra, I., Avila, J. D., Upadhyayula, M., & Bose, S. · International Journal of Extreme Manufacturing · 2023

Porous and functionally graded materials have seen extensive applications in modern biomedical devices—allowing for improved site-specific performance; their appreciable mechanical, corrosive, and biocompatible properties are highly sought after for lightweight and high-strength load-bearing orthopedic and dental implants.

Improving biocompatibility for next generation of metallic implants

Bandyopadhyay, A., Mitra, I., Goodman, S. B., Kumar, M., & Bose, S. · Progress in materials science · 2023

The increasing need for joint replacement surgeries, musculoskeletal repairs, and orthodontics worldwide prompts emerging technologies to evolve with healthcare's changing landscape. Metallic orthopaedic materials have a shared application history with the aerospace industry, making them only partly efficient in the biomedical domain. However, suitability of metallic materials in bone tissue replacements and regenerative therapies remains unchallenged due to their superior mechanical properties, eventhough they are not perfectly biocompatible.

Effects of Oxide Ceramic Addition on Biocompatibility of Titanium

Ciliveri, S., Mitra, I., Bose, S., Bandyopadhyay, A. · Metal-Matrix Composites. The Minerals, Metals & Materials Series · 2022

Titanium and its alloys are known for their excellent biocompatibility and mechanical performance and are used widely in load-bearing implant applications. However, titanium is bioinert, i.e., it does not help in bone–tissue interactions, thus not aiding in expedited patient healing. The inorganic phase of the bone contains macro-nutrients in trace elements such as Mg2+, Si4+, which play a vital role in bone formation and remodeling.

3D Printing in alloy design to improve biocompatibility in metallic implants

Mitra, I., Bose, S., Dernell, W.S., Dasgupta, N., Eckstrand, C., Herrick, J., Yaszemski, M.J., Goodman, S.B. and Bandyopadhyay, A. · Materials today · 2021

3D Printing (3DP) or additive manufacturing (AM) enables parts with complex shapes, design flexibility, and customization opportunities for defect specific patient-matched implants. 3DP or AM also offers a design platform that can be used to innovate novel alloys for application-specific compositional modifications. In medical applications, the biological response from a host tissue depends on a biomaterial's structural and compositional properties in the physiological environment.

3D Printing for Bone Regeneration

Bandyopadhyay, A., Mitra, I. & Bose, S. · Current Osteoporosis Reports · 2020

Three-dimensional printing (3DP) or additive manufacturing (AM) has transformed the manufacturing world in the past three decades—from product design/concept models to rapid prototyping and functional part manufacturing. 3DP is a layer-by-layer process that allows us to manufacture complex structures without any part-specific tooling. The first commercial 3DP technology, called “stereolithography,” was introduced by Charles Hull in 1988. Since then, different 3DP processes have been introduced commercially for a variety of materials and applications..

Electrically polarized TiO2 nanotubes on Ti implants to enhance early-stage osseointegration

Bandyopadhyay, A., Shivaram, A., Mitra, I., & Bose, S. · Acta biomaterialia · 2019

Ti is characteristically bioinert and is supplemented with modifications in surface topography and chemistry to find use in biomedical applications. The aim of this study is to understand the effects of surface charge on TiO2 nanotubes (TNT) on Ti implants towards early stage osseointegration.

Direct comparison of additively manufactured porous titanium and tantalum implants towards in vivo osseointegration

Bandyopadhyay, A., Mitra, I., Shivaram, A., Dasgupta, N., & Bose, S. · Additive Manufacturing · 2019

Material properties of implants such as volume porosity and nanoscale surface modification have been shown to enhance cell-material interactions in vitro and osseointegration in vivo. Porous tantalum (Ta) and titanium (Ti) coatings are widely used for non-cemented implants, which are fabricated using different processing routes. In recent years, some of those implants are being manufactured using additive manufacturing.

Synthesis of Chlorophyll Entrapped Red Luminescent Silica Nanoparticles for Bioimaging Application

Mitra, I., Manna, N., Manna, J. S., & Mitra, M. K. · Procedia Materials Science · 2014

A class of luminescent porous, spherical silica nanoparticles have been synthesized using simple oil-in-water microemulsion process in the size range of 15-50 nm evident from TEM and FESEM analysis. Mechanism of successful stabilization of chlorophyll molecule inside the nanoparticles has been evaluated by FTIR studies, and also supported by UV-Vis spectra.

Book Chapters

Additive Manufacturing of Cobalt-Chromium Alloy Biomedical Devices

Bandyopadhyay, A., Avila, J. D., Mitra, I., & Bose, S. · Additive Manufacturing in Biomedical Applications · ASM Handbook · 2022

This article discusses some of the additive manufacturing (AM) based fabrication of cobalt-chromium alloys and their respective mechanical, electrochemical, and in vivo performance.

CoCr Alloys

Bandyopadhyay, A., Traxel, K. D., Avila, J. D., Mitra, I., & Bose, S. · Biomaterials Science · Academic Press · 2020

Cobalt-base alloys are widely used in dental, knee, and hip arthroplasty applications because of their unique combination of high-strength, wear and corrosion resistance, and excellent fatigue resistance.